TYRE DEBRIS IN AQUATIC ENVIRONMENT: THE NEW BLACK?

TYRE DEBRIS IN AQUATIC  ENVIRONMENT: THE NEW BLACK?

Recently, models on the fate of tyre wear particles (TWPs) have estimated that 18% of TWP emissions are transported from roads to freshwater bodies and approximately 2% are led out to estuaries and then marine habitats. What then happens to the remaining 16% of TWP emissions left in the freshwater compartment is not yet clear

 

Louise Lynn Halle is a PhD student in Environmental Biology
at Roskilde University, Department of Natural Science and Environment, Denmark,
with funds from Danish Environmental Analysis

The presence of tyre wear particles (TWP) in the aquatic environment is considered an emerging contaminant, and one that has gained increasing interest during the past few years. Although the presence of TWPs in the environment is given greater attention these days, TWPs have probably been present since the dawn of the pneumatic car tyre production in the late 19th century. The first scientific report of tyre dust identification along a roadside was published in 1961. Different perspectives have since been applied to this field of research and almost decade by decade shifted foci from degradation patterns to heavy metal release, to impacts of scrap tyres on the aquatic environment and leaching of chemicals from tyres. More recently, research within this field has been directed towards repurposing scenarios using crumb rubber in turf fields and playground material. Finally, in the 2010s, micronised tyre rubber has become grouped with other polymer debris and hence become part of the polymer landscape usually referred to as ‘microplastics.’ TWPs are considered to represent the majority of microplastics (or polymer debris) in the environment, and the newest calculation on the wear of tyres is estimated at 0.81 kg per person per year.

Now, looking at TWPs through the lens of microplastic pollution, research and information from the microplastics field are very well applicable to TWPs in many instances. With this new perspective of TWPs, increasing awareness of possible adverse effects in the environment follows - how do TWPs distribute in the different environmental compartments (soil, air, sediment, water and biota (living organisms)) and how do TWPs behave when exposed to different abiotic factors in these environmental compartments. For example, UV-radiation or pH, temperature and salinity differences could affect TWPs, but to what degree? A recent paper on this very subject concluded that particularly temperature and mechanical stress could influence the toxicity of TWPs. The focus of tyre production and function have seemingly always been directed towards maximising the three hallmarks: grip, wear and rolling resistance, and rightfully so, but somewhere along the road we forgot to consider where tyre abrasion actually disappears to. Luckily, some scientists already thought of this and today we can begin to lay the foundation to our collected TWP knowledge, based on the available scientific literature.

 

From roads to water

Research shows that the minority of TWPs end up in the airborne fraction (0.1-10%) and recently TRWPs have been assessed to contribute a low risk to human health in the particulate matter (PM) PM2.5 and PM10 range. So, where to find the remaining 90.0-99.9% of tyre debris emissions? Early research on particulate distribution showed a decreasing concentration of TWPs with increasing distance from the road. From there, TWPs are expected to wash off during rainfalls, transporting them to different environmental compartments. Recently, models on the fate of TWPs have estimated that 18% of TWP emissions are transported from roads to freshwater bodies and approximately 2% are led out to estuaries and then marine habitats. What then happens to the remaining 16% of TWP emissions left in the freshwater compartment is not yet clear and more research is needed to answer this question.

Aquatic organisms living in the water column or the sediment can interact with TWPs in their natural habitats during this particle transportation through freshwater to the marine environment. Although there are no scientific references on field observations of TWP ingestion by aquatic biota yet, few recent observations of this behaviour under controlled laboratory settings have been reported. In 2009 the first observation of the water flea, Daphnia magna, ingesting TWPs was described in the scientific literature and only two years ago the first photos were published showing ingestion of TWPs in the benthic amphipod Gammarus pulex following sediment exposure. Shortly thereafter photos of TWP ingestion in the amphipod Hyalella azteca and opossum shrimps from the mysidae family followed after water-only exposures, and most recently freshwater and marine fish species have been documented ingesting TWPs under laboratory conditions.

The recent focus on particulate effects of TWPs on biota is still in its infancy and the latest development in this field investigates the possible effects of both the particulate fraction and the leachate fraction. The leachate fraction is the suite of chemicals that leach out from TWPs to the surrounding water. Previously, tyre toxicity investigations in the aquatic environment revolved solely around the leachate fraction, which has been the primary focus over the last 30 years. Among the first papers the effect of whole tyre leachate was investigated showing worn tyre leachate to exhibit greater toxicity than leachate from a pristine tyre to rainbow trout. Furthermore, decreasing toxicity was observed with increasing salinity indicating that salinity either influences the leachability of toxic constituents or that an interaction of salts and toxic chemicals is present. Exposure of shredded tyre chips to different bacteria likewise showed a correlation between decreasing toxicity and increasing salinity, concluding that tyre leachate is likely to be a greater threat to freshwater habitats than to estuarine or marine habitats.

Toxicity pattern

Mysid after ingestion of TWPs (Private photo)

Further testing of TWPs and leachate on a freshwater species recently showed a dissimilar toxicity pattern when comparing acute toxicity responses of TWPs or leachate. Here, the amphipod H. azteca was exposed to either TWPs in freshwater or the leachate fraction alone, i.e. with no particulates present. This showed that leachate was more toxic in lower concentrations, presumably because dissolved chemicals are more bioavailable. Although, at higher concentrations, the particle fraction of TWPs became more toxic. This phenomenon very well describes the complexity and discrepancies when working with TWPs in the aquatic environment. It is not just a question of determining toxicity of a single chemical under controlled settings, but rather investigating a mixture of many chemicals in changing ambient environments. This complex matrix of polymer and chemicals can be more or less bound to the particle, which in itself might have adverse effects. However, the particle could also function as a vessel, containing chemicals and making them more or less bioavailable depending on the surrounding environment. Discovering exactly which chemicals leach out under different exposure scenarios, and most importantly, what of that is actually bioavailable to aquatic living species is the more interesting question to answer.

Due to the amorphous nature of rubber, end-of-life tyres (ELTs) have been used as leachate collection material and been used to collect polycyclic aromatic hydrocarbons (PAHs) and metals from contaminated waters. This discrepancy between the different TWP uses that in some cases could deem toxic and have adverse effects but at the same time might serve to mitigate other environmental issues is a great conflict of contradictory traits. Now, we need to unravel exactly when these contradictory traits are possibly affecting aquatic environments negatively and when these traits might be used for our advantage.

 

So how do scientists quantify TWPs and chemical constituents or ‘biomarkers’ from TWP leachate in water? The quick answer is that no tried and tested procedure is more right than any other now, we simply do not have conformity or guidelines on how to do this. Especially when looking to find particulates from tyre debris, as this is not usually detected when investigating for other polymer debris e.g. microplastics. Therefore, it is expected that the total amount of microplastics has been underestimated due to the lack of data from TWPs, which make up a large part of the estimated microplastic load worldwide and have not been reported on a regular basis. A multitude of methods have been used to estimate TWP emissions by measuring the concentration of chemicals in samples, with more or less success over the years. The biomarkers that have been used to determine TWP concentration most successfully include quantification of benzothiazoles and zinc. Both chemicals are used as part of the vulcanisation process and are also ubiquitous in nature. They are used for manufacturing of other materials, but specific versions can be attributed mainly to tyre manufacturing and are thus the most reliable compounds to measure.

How this emerging field of tyre ecotoxicology will progress ultimately depends on cooperation between different stakeholders having a common goal to pursue. The one thing that we can probably all agree on, is the need for tyres and other rubber products in our society. How we then fill that need, and what future decisions we make to maximise our understanding of the possible negative implications of TWPs in the aquatic environment is of paramount importance. Our job now is to continue our research within this field and ultimately prevent excess and unnecessary pollution of the water bodies that we all depend on, in a manner that stays true to both the environment and our need for safe and reliable tyres. 

*The author is a PhD student in Environmental Biology at Roskilde University, Department of Natural Science and Environment, Denmark, with funds from Danish Environmental Analysis

 

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Rubber Tappers: Renew Group Insurance By July

The Rubber Board has announced that rubber tappers enrolled in the Group Insurance Cum Terminal Benefit Scheme, introduced in 2011-12, can renew their policies until 15 July 2025.

Policyholders are required to submit their current year’s contribution at their respective Rubber Board Regional Office. The scheme provides a coverage of INR 100,000 for natural death and up to INR 500,000 in the event of accidental death. A renewal notice has been dispatched to all members, but those who have not received the communication may treat this announcement as an official reminder.

Such individuals should promptly contact their nearest Rubber Board Regional Office to complete the payment process and ensure uninterrupted coverage. The Assistant Director (Publicity) has urged all eligible members to adhere to the deadline to avoid discontinuation of benefits.

Kuraray

The most basic difference between an electric vehicle (EV) and internal combustion engine (ICE) tyre is that the former demands lower rolling resistance, quieter tread patterns and higher load bearing capacity. While there have been innovations within the tyre industry to meet the current demand for EV tyres, at the molecular level, research and development continues to achieve enhanced compound efficiency as tyre mixtures are complex.

As electric vehicles redefine performance benchmarks, tyre technology is undergoing a molecular-level overhaul. While the industry has focused on rolling resistance, noise reduction and load capacity, Japan’s Kuraray is pushing the boundaries deeper into the chemistry of rubber itself. By integrating silane-functionalised liquid rubbers into natural rubber-silica systems, the company aims to resolve longstanding formulation challenges. These innovations not only offer measurable improvements in abrasion resistance and wet grip but also open the door to broader adoption of sustainable materials in EV tyres. Kuraray’s work signals a strategic shift towards more efficient, adaptable and environmentally aligned tyre compounds.

Japan-based chemicals manufacturer Kuraray has dismissed all odds to achieve a more efficient molecular chemistry in tyres with its silane-functionalised liquid rubbers. In an earlier issue, Tyre Trends had reported how the company’s silane-modified rubber marked a major leap in tyre technology as it enhanced polymer interaction within the tyre, especially in natural rubber and silica-based formulations.

Coming to the present, its silane-functionalised liquid rubbers offer the reduction of rolling resistance (RR) and the resulting compound shows excellent balance of low RR, abrasion resistance and wet grip performance.

Speaking to Tyre Trends exclusively on the development, Technical Service Engineer for Quality and Product Development Department, Elastomer Division, Kuraray Co., Naoto Takahashi, divulged, “We propose to incorporate natural rubber (NR) for silica-based PCR treads. NR is preferable for its high strength and from the viewpoint of sustainability. However, the combination of NR and silica has typically been considered unusual as compounds for PCR treads. One of the reasons is that NR and silica have poor interaction, which causes decrease of physical properties.”

“Our silane-functionalised liquid rubbers can react with silica in the mixing stage and with NR in the vulcanisation stage. Using this technology, NR or silica-based compounds have been proven to have an excellent balance of lower RR and competitive abrasion resistance and wet grip compared to typical styrene-butadiene rubber, butadiene rubber and silica compounds. So we believe it has the potential for EV tyres, which require these properties,” he added.

Furthermore, using silane-functionalised liquid rubber in tyre manufacturing offers several advantages. Firstly, it provides a plasticising effect during the mixing stage, leading to lower torque and electricity consumption.

Secondly, the improved rolling resistance itself contributes to the sustainability goals by extending the driving range of EVs. Long-range EVs significantly reduce carbon dioxide emissions compared to fossil fuel-powered vehicles. This helps mitigate global warming and other climate changes. In addition, EVs with extended range reduce the burden on charging infrastructure and promote efficient energy use. Less frequent charging means reduced strain on the power grid.

Additionally, the improved performance of NR and silica compounds sheds light on the utilisation of NR, which is a kind of sustainable material. “We believe this technology could expand the potential of NR. If you are considering using more NR in your products, then this type of liquid rubber could be useful,” added Takahashi.

MIXING THE MIXTURE

Typically, it has been said that conventional silane coupling agents have poor reactivity with NR. This is not the case for silane-functionalised liquid rubbers. The liquid rubbers react with silica at the mixing stage by hydrolysis and condensation, in the same manner as silane coupling agents. As a result, the silica would be surrounded by hydrophobic liquid rubber chains. This helps silica to disperse well in the rubber matrix.

In the subsequent stage of vulcanisation, the reaction of liquid rubber chains and NR occurs. This forms bonds between two types of rubbers, effectively resulting in reinforcement of silica-NR interaction.

“We believe that these mechanisms contribute to maximising the potential of NR and silica combination,” said Takahashi.

The molecular weight of rubber is another key factor in determining the characteristics of liquid rubbers, alongside the glass transition temperature and monomer components.

Explaining how the molecular weight range of Kuraray’s liquid rubbers affect its compatibility and performance in tyre applications, the executive said, “Our liquid rubbers’ molecular weight range is strategically positioned between typical plasticisers and solid rubbers, ensuring an optimal balance of enhanced processing and physical properties.”

“Each grade’s molecular weight is precisely controlled and tailored to specific purposes and applications. Generally, liquid rubbers with lower molecular weights offer superior compatibility with other ingredients, while those with higher molecular weights provide better physical properties. Interestingly, the viscosity of liquid rubber alone does not determine the processability of compounds. We are glad to support you in selecting the ideal grade of liquid rubber to achieve your objectives,” he added.

He also noted that liquid rubbers have a low tendency to bleed out as a plasticiser because of their higher molecular weight and ability to be vulcanised. The low migration property directly affects the life span of the tyres.

Additionally, the improved abrasion resistance compared to traditional plasticisers also offers the long-term liability of tyres. “Wear particle is one of the biggest issues in today’s tyre industry because it has been recognised that it has a severe impact on the environment. The new regulation to handle this matter has been under discussion for a long time. Our silane-functionalised liquid rubbers would offer the solution to these challenges,” noted Takahashi.

COMPETITIVE EDGE

One of the characteristics of the material is its narrow molecular weight distribution. This provides the benefit of suppressing reduced physical properties due to the low molecular weight fraction. Another is that it has functional groups grafted onto the polymer chain. These functional groups seem to have different reactivity compared to other types of modification.

These features have a positive effect on the storage stability and other performances as tyres. The company highlighted that it has already found that the material would not deteriorate so much for 1-2 years in a bulk container under air.

Besides, the silane-functionalised liquid rubber technology is applicable to various types of tyres including winter and all-season tyres, and high-performance tyres. It is particularly beneficial in improving the dispersion of silica fillers, reducing compound viscosity and enhancing overall tyre performance. This technology helps achieve a balance between grip, low RR and abrasion resistance, making it suitable for a wide range of tyre applications.

Considering the characteristics of the material, another application of this type of material is TBR. Most TBR tyres use NR and carbon black (CB) compounds with less or no oils. However, using silica in place of CB in TBRs is getting more and more attention to achieve the high level of rolling resistance and wet grip performance. Here emerges the problem of NR and silica combination. As mentioned above, the silane-functionalised liquid rubbers would act as the effective additive for these kinds of compounds.

Commenting on the role of the liquid rubbers in enhancing wet or ice grip performance on winter tyres, Takahashi explained, “We have two types of silane-functionalised liquid polybutadiene with relatively higher glass transition temperature (Tg) and lower Tg. Initially,

we only commercialised the former one. However, in response to customer demand, we have developed another grade with lower Tg and are now fully equipped to mass-produce.”

“Liquid rubbers with lower Tg provide flexibility to the compounds even at low temperatures, which is particularly beneficial for the ice-grip performance of winter tyres. This flexibility ensures that the rubber remains pliable and maintains good contact with icy surfaces, enhancing traction and safety. Since the compound Tg is also highly affected by other components such as solid rubbers, plasticisers and resins, we think that our product lineup with different Tg offers freedom of choice for users’ compound formulation,” he added.

MEETING DEMANDS

The company continuously spoke with tyre manufacturers during the development of its liquid rubber. “We have instruments in our laboratory for measuring not only compound properties but also tyre performances such as wet grip and abrasion resistance. This allows us to have close and detailed technical communication with our customers,” said Takahashi.

He added, “The wet grip performance is usually expressed by the value of tanδ at 0 deg.C as an index from the viscoelasticity measurement. But the actual compound’s grip performance often shows a different result from the viscoelasticity. We have equipment to measure the friction coefficient of compounds on wet and icy surfaces, allowing us to minimise the discrepancy between viscoelasticity and grip performance.”

Alluding to how the use of silane-functionalised liquid rubber in EV tyres aligns with current trends and future directions in tyre technology, he said, “We recognise the growing trend towards sustainability as well as the importance of reducing rolling resistance and wear particles. Here, we recommend using NR more to address these issues. While the combination of NR and silica may not be the conventional choice for PCR tread compounds, we believe that our innovative approach demonstrates the potential of this formulation. The use of silane-functionalised liquid rubber offers the excellent dispersion and reinforcement of NR and silica compounds, paving the way for the solution to address future challenges in tyre technology.”

Takahashi indicated that the silane-functionalised liquid rubber can play a role in reducing the carbon footprint of tyre production. The key driver, he explained, is a measurable drop in rolling resistance, which translates into lower fuel consumption for internal combustion vehicles and reduced electricity use in EVs.

The firm also highlighted its broader sustainability efforts, noting that its liquid rubber plant is ISCC Plus-certified. From this year, Kuraray has started producing sustainable materials under a mass-balance approach – an initiative that includes its latest silane-functionalised grades, though the product range is still expanding.

On managing cost-performance trade-offs, he acknowledged that liquid rubber typically commands a higher price than traditional plasticisers. However, the benefits tend to supplement the cost.

The company pointed to challenges like dispersing high-surface-area silica in tread compounds – an area where its liquid rubber grades can provide a processing advantage. It also emphasised the potential of NR and silica combinations, made feasible with its silane-modified products, as an example of how formulation innovation can justify the premium.

Kuraray’s silane-functionalised liquid rubber represents a critical inflection point for tyre formulation – technically and environmentally. By enabling stable silica dispersion in natural rubber and forming durable crosslinks during vulcanisation, it addresses both performance and sustainability imperatives.

While the cost remains a consideration compared to traditional plasticisers, the material’s added value, such as reduced energy use, lower rolling resistance and extended tyre life, could redefine return on investments calculations for manufacturers. Its compatibility with evolving regulations on wear particles and carbon footprint reduction positions it not just as an additive but as a strategic material. The challenge ahead lies in scaling adoption without compromising economic efficiency.

Apollo Tyres Hungary Plant Gets ISCC+ Certification

Apollo Tyres Hungary Plant Gets ISCC+ Certification

Apollo Tyres, one of the leading tyre manufacturers in the world, has added another feather to its cap, with its Hungary production plant bagging the International Sustainability and Carbon Certification Plus (ISCC+) certification.

The globally recognised ISCC certification is a voluntary programme that recognises companies for their sustainability and carbon reduction initiatives. Apollo Tyres, by achieving ISCC+ certification, has been recognised for not only meeting the stringent sustainability standards but also for its responsible production in the industry.

Apollo Tyres Secures Gold Medal In 2025 EcoVadis Sustainability Rating

As part of its commitment, the tyre maker continues to focus on monitoring and verifying sustainability practices across its processes and supply chain.

Rajeev Kumar Sinha, Chief Manufacturing Officer, Apollo Tyres, said, “This certification is an important step forward as we continue to integrate sustainability deeply into our operations. It aligns perfectly with our ambitious goal of incorporating 40 percent sustainable raw materials – including renewable and recycled input materials – into our products by 2030.”

Kraton Corporation Publishes 2024 Sustainability Report

Kraton Corporation, a global leader in speciality polymers and biobased solutions derived from pine wood pulping co-products, has published its 2024 Sustainability Report, ‘Innovating with Purpose’. The report showcases the company’s advancements in climate action, circular product innovation and value chain partnerships, reinforcing its commitment to sustainable solutions.

Key achievements include a 41 percent reduction in Scope 1 & 2 greenhouse gas emissions since 2014 and a 35 percent decline in emissions intensity. Kraton also maintained its EcoVadis Platinum rating for the fourth consecutive year and received the 2024 Nitto Supplier Sustainability Award. Strategic initiatives such as a Double Materiality Assessment and a USD 35 million investment in biorefinery upgrades at its Panama City facility further demonstrate Kraton’s sustainability leadership.

The company enhanced transparency by expanding life cycle assessment (LCA) data to cover nearly 90 percent of its product portfolio, helping customers evaluate environmental impacts. Additionally, Kraton launched a data excellence program to streamline ESG reporting and refine decarbonisation goals.

Aligned with GRI, SASB, UN Global Compact and TCFD frameworks, the report reflects Kraton’s sustainability pillars: Being Reliable Partners, Preserving Planet and Empowering People. These efforts underscore Kraton’s dedication to driving meaningful progress across its operations and industries.

Marcello Boldrini, Kraton Chief Executive Officer, said, “2024 marked a pivotal year in Kraton’s sustainability journey. We turned ambition into action, significantly reducing our Scope 1 and 2 emissions by 41 percent from our 2014 baseline and earned an EcoVadis Platinum rating for the fourth consecutive year. We accelerated our decarbonisation strategy, advanced biobased innovation and partnered with customers such as WJ Group and Henkel to help address global sustainability challenges. As demand for sustainable chemicals grows, our focus remains on developing the right solutions, fostering strong partnerships and cultivating the culture necessary to lead this transformation responsibly and competitively.”

Rogier Roelen, Kraton Chief Sustainability Officer, said, “We have established new processes to scale credible, data-driven sustainability across our business. In 2024, we enhanced our ESG reporting through a data harmonisation programme and completed a Double Materiality Assessment to better align with the Corporate Sustainability Reporting Directive (CSRD). We also expanded our Life Cycle Assessment (LCA) data to cover almost 90 percent of our product portfolio, providing customers with greater transparency into the environmental impact of our products. These efforts reinforce our ability to identify where we can make the most impact and support more informed, strategic decision-making.”